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An Introductory Course of Quantitative Chemical Analysis With Explanatory Notes   By:

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[Transcriber's notes: In the chemical equations, superscripts are indicated with a ^ and subscripts are indicated with a . The affected item is enclosed in curly brackets {}. Examples are H^{} for hydrogen ion and H {2}O for water. Since the underscore is already being used in this project, italics are designated by an exclamation point before and after the italicized word or phrase.]












This Introductory Course of Quantitative Analysis has been prepared to meet the needs of students who are just entering upon the subject, after a course of qualitative analysis. It is primarily intended to enable the student to work successfully and intelligently without the necessity for a larger measure of personal assistance and supervision than can reasonably be given to each member of a large class. To this end the directions are given in such detail that there is very little opportunity for the student to go astray; but the manual is not, the author believes, on this account less adapted for use with small classes, where the instructor, by greater personal influence, can stimulate independent thought on the part of the pupil.

The method of presentation of the subject is that suggested by Professor A.A. Noyes' excellent manual of Qualitative Analysis. For each analysis the procedure is given in considerable detail, and this is accompanied by explanatory notes, which are believed to be sufficiently expanded to enable the student to understand fully the underlying reason for each step prescribed. The use of the book should, nevertheless, be supplemented by classroom instruction, mainly of the character of recitations, and the student should be taught to consult larger works. The general directions are intended to emphasize those matters upon which the beginner in quantitative analysis must bestow special care, and to offer helpful suggestions. The student can hardly be expected to appreciate the force of all the statements contained in these directions, or, indeed, to retain them all in the memory after a single reading; but the instructor, by frequent reference to special paragraphs, as suitable occasion presents itself, can soon render them familiar to the student.

The analyses selected for practice are those comprised in the first course of quantitative analysis at the Massachusetts Institute of Technology, and have been chosen, after an experience of years, as affording the best preparation for more advanced work, and as satisfactory types of gravimetric and volumetric methods. From the latter point of view, they also seem to furnish the best insight into quantitative analysis for those students who can devote but a limited time to the subject, and who may never extend their study beyond the field covered by this manual. The author has had opportunity to test the efficiency of the course for use with such students, and has found the results satisfactory.

In place of the usual custom of selecting simple salts as material for preliminary practice, it has been found advantageous to substitute, in most instances, approximately pure samples of appropriate minerals or industrial products. The difficulties are not greatly enhanced, while the student gains in practical experience.

The analytical procedures described in the following pages have been selected chiefly with reference to their usefulness in teaching the subject, and with the purpose of affording as wide a variety of processes as is practicable within an introductory course of this character. The scope of the manual precludes any extended attempt to indicate alternative procedures, except through general references to larger works on analytical chemistry. The author is indebted to the standard works for many suggestions for which it is impracticable to make specific acknowledgment; no considerable credit is claimed by him for originality of procedure... Continue reading book >>

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